石油化工设备技术 ›› 2023, Vol. 44 ›› Issue (5): 33-39.doi: 10.3969/j.issn.1006-8805.2023.05.007

• 状态监测与分析 • 上一篇    

P12耐热钢蠕变微观组织演化研究及寿命预测分析

杨家兵   

  1. 中韩(武汉)石油化工有限公司,湖北 武汉 430082
  • 收稿日期:2023-06-25 接受日期:2023-08-30 出版日期:2023-09-15 发布日期:2023-09-11
  • 作者简介:杨家兵,男,1986年毕业于武汉化工学院化工机械专业,学士,主要从事静设备管理工作,高级工程师。

Study on Creep Microstructure Evolution and Life Prediction of P12 Heat-resistant Steel

Yang Jiabing   

  1. SINOPEC Tenth Construction Co., Ltd., Qingdao, Shandong, 266555
  • Received:2023-06-25 Accepted:2023-08-30 Online:2023-09-15 Published:2023-09-11

摘要: 为探究P12耐热钢蠕变断裂机理,对P12耐热钢在630 ℃、70 MPa应力条件下进行了一系列不同加载时间的蠕变试验,然后对蠕变后的试样进行金相显微组织检测和扫描电镜分析,以获得其高温蠕变过程中微观组织的演化情况,同时结合计算机图像处理技术对P12耐热钢在蠕变条件下的碳化物析出和珠光体球化程度进行了定量分析。分析结果表明:蠕变时间的延长会加剧P12耐热钢碳化物析出程度,一方面碳化物的数量不断增多,另一方面碳化物的尺寸也随之增大;而珠光体球化级别也随蠕变时间的累积而加剧,蠕变时间为360 h时,珠光体球化级别即高达3级;此外,珠光体组织中的渗碳体数量和尺寸随蠕变的加剧而急剧减小。蠕变过程中,P12耐热钢微观组织的劣化或将是其蠕变断裂的重要因素。文章还对P12高温蒸汽管道进行寿命预测以及高温持久试验,确定了P12耐热钢的Manson-Haferd参数PMH(σ)与应力σ之间的关系,并基于Manson-Haferd参数法预测出应力σ为43.15 MPa、服役温度为520 ℃的P12高温蒸汽管道的服役寿命为19.98万h。

关键词: P12耐热钢, 蠕变断裂, 微观组织, 组织演化, 寿命预测, Manson-Haferd参数法

Abstract: In order to explore the creep fracture mechanism of P12 heat-resistant steel, a series of creep tests were carried out on P12 heat-resistant steel under 630 ℃ and 70 MPa stress conditions. Then the creeped specimens were examined by metallographic microscopy and analyzed by scanning electron microscopy to obtain the microstructure evolution during high temperature creep. And the level of carbide precipitation and pearlite spheroidization of P12 heat-resistant steel under creep was quantitatively analyzed by combining computer image processing technology. The results show that the prolongation of creep time increases the precipitation of carbides in P12 heat-resistant steel. On the one hand, the amount of carbides increases continuously, on the other hand, the size of carbides increases accordingly. The level of pearlite spheroidization also increases with the accumulation of creep time. When the creep time is 360 hours, the level of pearlite spheroidization is up to grade 3. In addition, the amount and size of cement carbon in the pearlite structure decreases sharply with the increase of creep time. The deterioration of the microstructure of P12 heat-resistant steel during creep may be an important factor for its creep fracture. In order to predict the service life of P12 high-temperature steam pipe, a series of high-temperature endurance tests were carried out to determine the relationship between Manson-Haferd parameter PMH(σ) and stressσ of P12 heat-resistant steel. Then Based on the Manson-Haferd parameter method, the service life of P12 high-temperature steam pipe with stress σ of 43.15 MPa and service temperature of 520 ℃ is predicted to be 199.8 thousand hours.

Key words: P12 heat-resistant steel, creep rupture, microstructure, structural evolution, life prediction, Manson-Haferd parameter method